Das, Nandini and Bhattacharya, Dipten and Sen, Amarnath and Maiti, Himadri Sekhar (2009) Sonochemical synthesis of LaMnO(3) nano-powder. Ceramics International, 35 (1). pp. 21-24. ISSN 0272-8842
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Abstract
We report the preparation of LaMnO(3) nanosized powder by the sonochemical process. Sodium dodecyl sulphate (SDS) was used as surfactant, to prevent agglomeration. The particle size obtained in this method was 19-55 nm. The phase formation temperature of LaMnO(3) was 700 degrees C which is lower than other conventional processes. So sonochemical process is cost effective and it is more acceptable considering its ease of preparation in comparison to other conventional processes. Powder synthesized was characterized by measuring crystallite size, specific surface area, morphology and by thermal analysis. The particle sizes of the powders were controlled by calcinations schedule. Narrow size distribution and core and shell structure of the prepared powder was revealed by transmission electron microscopy. (C) 2007 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
Item Type: | Article |
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Uncontrolled Keywords: | Sonochemical; LaMnO(3); Nano-particle; TEM |
Subjects: | Electronics |
Divisions: | UNSPECIFIED |
Depositing User: | Ashok K Podder |
Date Deposited: | 22 Feb 2012 06:28 |
Last Modified: | 22 Feb 2012 06:28 |
URI: | http://cgcri.csircentral.net/id/eprint/991 |
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