Kundu, Dipali and Roy, S K (1989) Spectrophotometric determination of silica in barium titanate and zirconia ceramics after extraction of silicomolybdate on polyurethane foam. Transactions of the Indian Ceramic Society, 48 (3). pp. 47-49. ISSN 0371-750X

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Abstract

A spectrophotometric method has been developed for the determination of trace amounts of silica in barium titanate and zirconia ceramics based on the formation of molybdosilicic acid, its preconcentration on polyurethane foam, elution in acetone (acetone: HCl = 99:1) and reduction to molybdenum blue form. The method is applicable up to 2 μg Si/ml. The minimum that was detected by this method was 5.0 ng Si/ml. The method yielded agreeable results.

Item Type: Article
Subjects: Microstructure and Characterization
Engineering Materials
Divisions: UNSPECIFIED
Depositing User: Bidhan Chaudhuri
Date Deposited: 06 Dec 2013 12:23
Last Modified: 05 Mar 2016 13:37
URI: http://cgcri.csircentral.net/id/eprint/2446

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